A critical study of the determination of molybdenum in plant material
- Authors: Gore, William Tompson
- Date: 1961
- Subjects: Molybdenum , Plants -- Analysis , Spectrophotometry , Polarography
- Language: English
- Type: Thesis , Masters , MSc
- Identifier: vital:4477 , http://hdl.handle.net/10962/d1012071 , Molybdenum , Plants -- Analysis , Spectrophotometry , Polarography
- Description: 1. Polarographic and spectrophotometric methods for the determination of molybdenum were reviewed. 2. The inclusion of salicylaldoxine in several supporting electrolytes was examined with a view to developing a polarographic procedure, suitable for routine analyses, which did not necessitate a preliminary time-consuming separation stage. A stable molybdenum wave was obtained from an electrolyte having a composition similar to the test solution obtained after the wet digestion of plant material. The height of the wave was found to be, over an optimum range, independent of the reagent concentrations. The wave was however distorted by a maximum, which rendered it unsuitable for quantitative analytical application. 3. The spectrophotometric procedure for molybdenum using thiocyanate is virtually specific and was examined critically. Modifications were found to improve the sensitivity of the procedure, and the stability of the chromatic compound. 4. The modified spectrophotometric procedure is recommended for the routine determination of molybdenum in plant material.
- Full Text:
- Authors: Gore, William Tompson
- Date: 1961
- Subjects: Molybdenum , Plants -- Analysis , Spectrophotometry , Polarography
- Language: English
- Type: Thesis , Masters , MSc
- Identifier: vital:4477 , http://hdl.handle.net/10962/d1012071 , Molybdenum , Plants -- Analysis , Spectrophotometry , Polarography
- Description: 1. Polarographic and spectrophotometric methods for the determination of molybdenum were reviewed. 2. The inclusion of salicylaldoxine in several supporting electrolytes was examined with a view to developing a polarographic procedure, suitable for routine analyses, which did not necessitate a preliminary time-consuming separation stage. A stable molybdenum wave was obtained from an electrolyte having a composition similar to the test solution obtained after the wet digestion of plant material. The height of the wave was found to be, over an optimum range, independent of the reagent concentrations. The wave was however distorted by a maximum, which rendered it unsuitable for quantitative analytical application. 3. The spectrophotometric procedure for molybdenum using thiocyanate is virtually specific and was examined critically. Modifications were found to improve the sensitivity of the procedure, and the stability of the chromatic compound. 4. The modified spectrophotometric procedure is recommended for the routine determination of molybdenum in plant material.
- Full Text:
A critical study of methods for the determination of zinc in soils and plant materials
- Authors: Eve, Desmond John
- Date: 1955
- Subjects: Soils -- Zinc content , Soils -- Analysis , Plants -- Analysis
- Language: English
- Type: Thesis , Masters , MSc
- Identifier: vital:4468 , http://hdl.handle.net/10962/d1011770 , Soils -- Zinc content , Soils -- Analysis , Plants -- Analysis
- Description: Although it is only fairly recently that the importance of trace elements in plant nutrition has been established, enormous advances have been made in this field of research and numerous publications of considerable scientific and economic importance, dealing with the subject, have appeared. The physiological functions of zinc in promoting plant growth have not all been satisfactorily identified as yet. There are indications, however, that zinc acts as a catalyst or regulator in plant metabolism. It appears too, that the element plays some role in chlorophyll formation. Zinc deficiency is associated with leaf chlorosis and a general collapse of v ital processes. The analysis of leaves and soils has become an essential part of the study of the nutritional diseases of plants and it is imperative that accurate and reliable methods of analysis should be available. Intro. p. 1.
- Full Text:
- Authors: Eve, Desmond John
- Date: 1955
- Subjects: Soils -- Zinc content , Soils -- Analysis , Plants -- Analysis
- Language: English
- Type: Thesis , Masters , MSc
- Identifier: vital:4468 , http://hdl.handle.net/10962/d1011770 , Soils -- Zinc content , Soils -- Analysis , Plants -- Analysis
- Description: Although it is only fairly recently that the importance of trace elements in plant nutrition has been established, enormous advances have been made in this field of research and numerous publications of considerable scientific and economic importance, dealing with the subject, have appeared. The physiological functions of zinc in promoting plant growth have not all been satisfactorily identified as yet. There are indications, however, that zinc acts as a catalyst or regulator in plant metabolism. It appears too, that the element plays some role in chlorophyll formation. Zinc deficiency is associated with leaf chlorosis and a general collapse of v ital processes. The analysis of leaves and soils has become an essential part of the study of the nutritional diseases of plants and it is imperative that accurate and reliable methods of analysis should be available. Intro. p. 1.
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